Ethanol will boil at *90f under full vacuum
i use 150f to boil it off slowly into the open air (outside) then i reduce to 120f for a long purge full vac
All temps with IR thermometer
Everclear is illegal in my state. Is it worth ordering some 99% ISO online versus just using the 91% thats cheap and available here? From what you guys are describing the everclear evaporates alot easier than the 91% ISO. Anyone used both and have any insight?
ethanol residuals are more salubrious
East coasters check out, http://www.winechateau.com/
West coasters, try http://organicalcohol.com/store/
Hello all
My new toy just arrived 2000ml filter flask and 1000ml funnel. I am ignorant in lab glass and when I ordered the funnel I was unaware that in stead of holes it has something like a porous stone and I have no idea if it will let the concentrate pass through it.
When I poured some Iso in it it wouldn't drip through until through until I used the hand help vacuum pump. It looks like it will be hell to keep this stone clean. Will it let the concentrate pass through?
[URL=https://www.icmag.com/ic/picture.php?albumid=40691&pictureid=1702063&thumb=1]View Image[/url] [URL=https://www.icmag.com/ic/picture.php?albumid=40691&pictureid=1702065&thumb=1]View Image[/url] [URL=https://www.icmag.com/ic/picture.php?albumid=40691&pictureid=1702064&thumb=1]View Image[/url] [URL=https://www.icmag.com/ic/picture.php?albumid=40691&pictureid=1702066&thumb=1]View Image[/url]
Everclear is illegal in my state. Is it worth ordering some 99% ISO online versus just using the 91% thats cheap and available here? From what you guys are describing the everclear evaporates alot easier than the 91% ISO. Anyone used both and have any insight?
Ok I got to try out my funnel and flask. What I like about it is I can pour the Iso and material right into a simple kitchen strainer right into the funnel.
Skyhighler's idea of using the coffee filter was spot on it keeps the filter paper from floating up.
Ok now for the bad part the hand held vacuum pump sucks well actually it doesn't suck. I pumped as fast as I could and could only generate 100 mmHG ( according to the gauge) I got close to 200 once but for a very short time.
I was running shake and popcorn and there are a lot of fines and they clog up everything very quickly and you cant get the hand held vacuum to pull hard enough to get anything but a dribble after awhile.
I am disappointed now its back to researching something different for the vacuum pump.
SkyHighler
Timboy recommended that also but here in the midwest running the water in the winter outside is a problem and I don't have a water spigot in my garage and the better half doesn't want me to do this in the house.
What did you think about the air pump vacuum I posted?
Prefilter it with something like a bandana or a scrap piece of a clean tshirt or terry towel
http://www.homedepot.com/p/HDX-Terry-Towels-20-Pack-7-620/203299415
That is a very fine filter (the buchner) so you need to prefilter if the material is dirty. Another option would be paint strainer
http://www.homedepot.com/p/HDX-1-gal-Elastic-Top-Strainers-2-Pack-11572-36WF/202061359
Timboy
Great advice I will prefilter the shake/popcorn mix.
Tell me about your experience with the water siphon vacuum pump?
How strong is the stream of Iso through the filter?
SkyHighler
Ok just had a little time to look at this. The commercial device in your link has a 0.7 cfm capability will this provide evacuation needed? This is not a closed vacuum system my assumption is that higher cfms are required but I have no idea other than gut feel to quantify this.
I researched water fountain pumps and they are inexpensive but not sure if I can generate the required cfm needed to pull through the clogged filter on my funnel?
Have you used this system before ?